TY  - THES
N1  - Pembimbing :  Retno Rahmawati, M.Si

ID  - digilib14353
UR  - https://digilib.uin-suka.ac.id/id/eprint/14353/
A1  - SRI SUSANTI,  NIM. 07620006
Y1  - 2014/07/03/
N2  - This study aims to obtain nano-sized magnetite nanoparticles and study the effect
of temperature on the function of the crystal structure of magnetite nanoparticles.
Synthesis is done by mixing natural sand with HCl as solvent and NaOH as a
precipitant ultrasonic. Function of temperature was varied from 30? C, 50? C, and
80? C and seen its effect on the cubic crystal structure formed from the sample.
Sample test results magnetite nanoparticles were characterized by using XRD (XRay
Difraction) to determine the phase formation and the size of the crystals
formed and SEM (Scanning Electron Microscope) to determine the morphology
of the sample. From the results of the characterization of unknown fraction of the
sample volume decreases due to the appearance of another phase in the form (?-
Fe2O3), in addition to the sample of magnetite nanoparticles have a face-centered
cubic structure (Face Centered Cubic) with the crystal fields in accordance with
the standard crystal field JCPDS (Joint Committee of Powder standart) no.19-629
with the size of crystals at temperatures 30? C of (22.62 ± 1.56) nm, at a
temperature of 50? C (24.30 ± 1.20) nm, and the temperature of 80? C (20 , 60 ±
0.60) nm. The results showed that the sonochemical method with a function of
temperature can reduce the size of magnetite nanoparticles and no effect on the
crystal structure of magnetite nanoparticles.


PB  - UIN SUNAN KALIJAGA
KW  - Keyword : Magnetite Nanoparticles
KW  -  Temperature On The Function
KW  -  The Crystal
Structure




M1  - skripsi
TI  - KAJIAN STRUKTUR KRISTAL NANOPARTIKEL MAGNETITE (Fe3O4)
SEBAGAI FUNGSI TEMPERATUR DARI HASIL SINTESIS DENGAN
MENGGUNAKAN METODE SONOKIMIA

AV  - restricted
ER  -