eprintid: 46857
rev_number: 10
eprint_status: archive
userid: 12259
dir: disk0/00/04/68/57
datestamp: 2021-11-17 04:06:22
lastmod: 2021-11-17 04:06:22
status_changed: 2021-11-17 04:06:22
type: thesis
metadata_visibility: show
creators_name: Apriani Rahayu, NIM. 14630003
title: SINTESIS SENYAWA N-(HIDROKSIFENIL)-3,4-DIMETOKSIBENZAMIDA MELALUI REAKSI AMIDASI 3,4-DIMETOKSIBENZALDEHID DENGAN P-AMINOFENOL
ispublished: pub
subjects: KC
divisions: jur_kim
full_text_status: restricted
keywords: Amidation, oxidation, p-aminophenol
note: Dr. Susy Yunita Prabawati, M.Si
abstract: Synthesis of the compound n-(hydroxyphenyl)-3,4-dimethoxybenzamide
through the amidation reaction of 3,4-dimethoxybenzaldehyde with p-aminophenol
has been carried out. The purpose of this study was to synthesize and characterize
p-aminophenol derivatives using 3,4-dimethoxybenzaldehyde and to determine the
characteristics of n-(hydroxyphenyl)-3,4-dimethoxybenzamide using IR spectrophotometer, UV-vis spectroscopy and mass spectroscopy. The compound n-(hydroxyphenyl)-3,4-dimethoxybenzamide was synthesized through an amidation reaction between an aldehyde compound in the form of 3,4- dimethoxybenzaldehyde and an amine in the form of p-aminophenol. The synthesized product was identified by melting point, IR spectrophotometer, UV-Vis spectroscopy and mass spectroscopy. The results of the study were chocolate crystals with a melting point of 163°C and a percentage yield of 43%. The results of the characterization of the compound N-(hydroxyphenyl)-3,4-dimethoxybenzamide using the UV-Vis instrument resulted in an absorption peak of wavelength (α) 236 nm. The results of FTIR identification resulted in a vibrational absorption of the carbonyl group (-C=O) on the amide in the absorption region of 1620 cm-1, strengthened by absorption in the area of 3340 cm-1 and 3278 cm-1, there was a double amide peak indicating the presence of a -NH group. MS identification results showed the molecular weight of the product was 109.13 g/mol.
date: 2021-08-25
date_type: published
pages: 56
institution: UIN SUNAN KALIJAGA YOGYAKARTA
department: FAKULTAS SIANS DAN TEKNOLOGI
thesis_type: skripsi
thesis_name: other
citation:   Apriani Rahayu, NIM. 14630003  (2021) SINTESIS SENYAWA N-(HIDROKSIFENIL)-3,4-DIMETOKSIBENZAMIDA MELALUI REAKSI AMIDASI 3,4-DIMETOKSIBENZALDEHID DENGAN P-AMINOFENOL.  Skripsi thesis, UIN SUNAN KALIJAGA YOGYAKARTA.   
document_url: https://digilib.uin-suka.ac.id/id/eprint/46857/1/14630003_BAB-I_IV-atau-V_DAFTAR-PUSTAKA1.pdf
document_url: https://digilib.uin-suka.ac.id/id/eprint/46857/2/14630003_BAB-II_sampai_SEBELUM-BAB-TERAKHIR.pdf