@phdthesis{digilib7331,
           month = {November},
           title = {SINTESIS DAN KARAKTERISASI SURFAKTAN N-METIL
GLUKAMIDA DARI N-METIL GLUKAMINA
DENGAN MINYAK JELANTAH SAWIT
},
          school = {UIN SUNAN KALIJAGA},
          author = {NIM: 08630031 TITIK PURWANINGSIH },
            year = {2012},
             url = {https://digilib.uin-suka.ac.id/id/eprint/7331/},
        abstract = {N-methyl glukamide surfactant has been synthesized from waste cooking oil
and N-methyl glukamine. Were synthesized via indirect amidation of methyl ester
used frying oil. Products was carried out by FT-IR and Furthermore, N-methyl
glukamide as synthetic product was characterized as surfactant.
Transesterification of used frying oil with base catalyst (NaOH) produced
mixture of methyl ester, Le methyl ester in 94,42\%. From mixture of methyl ester,
i.e methyl ester of palmitate, oleate, isostearate, and trans-9-octadecinoic acid
withpercent conversion 33,28\%. Amidation of methyl esters with N-methyl
glukamine (2:3) for 3 h produced the related N-methyl glukamide in 90.49\%.
Characterization as surfactant showed that the N-methyl glukamide could
reduced the surface tension of water from 65,2 mN/m to16,27 mN/m. Foam was
stable until 1.5 hours of observed time, petrol-water- palm oil and surfactant system
has 100 \% emulsion index, stability emulsions have observed until 4 days. Further
more, HLB value of surfactant is 8,045 with characteristic dispersion in the water
and can be applied as metting agent.
Key words: Surfactant, N-methyl glukamide, HLB value (Hydrophyle Lypophyle
Balance)

}
}